Ceramics-Silikáty 55, (3) 240 - 245 (2011) |
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PROPERTIES OF Al₂O₃ FOAMS OPTIMIZED BY FACTORIAL DESIGN |
Bazelová Zora, Pach Ladislav, Lokaj Ján,
Kovár Vladimír |
Department of Ceramics, Glass and Cement, Faculty of Chemical and Food Technology,
Slovak Technical University, Radlinského 9, Bratislava, Slovakia
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Keywords: Alumina foam, Ceramic, Bulk density, Compressive strength |
Alumina foam was prepared by the direct foaming method. The foam was stabilized by in situ partially hydrophobized
particles of Al₂O₃. Dodecylbenzenesulphonic acid was used for hydrophobization and it also acted as a foaming agent. The
composition of the starting suspensions (Al₂O₃, boehmite, dodecylbenzenesulphonic acid and water) were varied according
to factorial design. The resulting properties observed were: foam ratio, foam shrinkage on drying and sintering, bulk density
and porosity of ceramic foams, average pore size and compressive strength. The final properties of foams dependent on
statistically significant factors (boehmite, dodecylbenzenesulphonic acid) were evaluated by common software. The foam
ratio decreased and the bulk density of the alumina foams increased with increasing quantity of the dodecylbenzenesulphonic
acid (0.1-0.2 wt.%). Bulk density of alumina foams ranged from 88 to 155 kg/m³
and average pore size reached 111 μm to
215 μm depending on the quantity of the dodecylbenzenesulphonic acid. The microstructure of ceramic foams reached high
porosities ranging from 96 to 98 %. The compressive strength of the alumina foams increased with increasing quantity of
boehmite (1-3 wt.%) and it reached values of 333 kPa. |
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