Ceramics-Silikáty 57, (3) 185 - 189 (2013) |
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MONOCLINIC ZIRCONIA SINTERED BODIES PREPARED VIA TWO-STEP SINTERING AND CHARACTERISATION OF SELECTED MECHANICAL PROPERTIES |
Wójtowicz B., Pyda W., Łabuz A. |
AGH University of Science and Technology, Faculty of Material Science and Ceramics,
Department of Ceramics and Refractories, A. Mickiewicz Av. 30, 30-065 Kraków, Poland
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Keywords: Unstabilised zirconia sinters, Monoclinic zirconia sinters, Two step sintering, Mechanical properties |
In the paper we examine some mechanical properties of the unstabilised zirconia sinters, such as Vickers hardness and
fracture toughness. The sinters were prepared using two step sintering technique. It is the first time, when two step sintering
is used to process unstabilised zirconia nanopowders. As a preparatory experiment, a microstructure evolution of the sinters
was determined in order to select the temperatures T1 and T2 of two step sintering. The samples were sintered below the
monoclinic to tetragonal transformation temperature, using several T1 and T2 combinations and different sintering times. The
sinters were compared in terms of density, grain size, Vickers' hardness and fracture toughness. The samples were sintered to
full density, showing a grain size of 95 nm, Vickers hardness of 11 GPa and fracture toughness of 5.32 MPa∙m0.5. |
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